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First Use of a Mineral Liquid Crystal for Measurement of Residual Dipolar Couplings of a Nonlabeled Biomolecule

✍ Scribed by Hervé Desvaux; Jean-Christophe P. Gabriel; Patrick Berthault; Franck Camerel

Book ID
101376814
Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
177 KB
Volume
40
Category
Article
ISSN
0044-8249

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Simultaneous determination of 1H–1H and 1H–13C residual dipolar couplings in a chiral liquid crystal solvent using a natural abundance HSQC experiment
✍ Vasilios M. Marathias; Igor Goljer; Alvin C. Bach II 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 186 KB

## Abstract A high‐resolution, phase‐sensitive, natural abundance __F__~2~‐coupled ^1^H–^13^C HSQC (F2HSQC) NMR experiment was developed to measure simultaneously both ^__n__^__D__~HH~ and ^1^__D__~CH~ residual dipolar couplings (RDCs) of small molecules present in a chiral polypeptide liquid cryst