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First Synthesis of 3′-Deoxy Lewisx Pentasaccharide.

✍ Scribed by Chafika Gourmala; Zhenyuan Zhu; Yun Luo; Bo Tao Fan; Said Ghalem; Yongzhou Hu; Yongmin Zhang

Book ID
101984647
Publisher
John Wiley and Sons
Year
2005
Weight
8 KB
Volume
36
Category
Article
ISSN
0931-7597

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✍ Daniel H. Murray; J. Prokop 📂 Article 📅 1965 🏛 John Wiley and Sons 🌐 English ⚖ 340 KB

Condensation of Z-deoxy-~-ribose with nitromethane gave, after deionization, a syrupy mixture of epimeric l-nitro-1,3-dideoxy-hexitols. Acid hydrolysis under Nef reaction conditions produced a mixture of 3-deoxy-~-glucose and 3-deoxy-m mannose, separable by cellulose chromatography or fractional cry