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First Anhydrous Gold Perchlorato Complex: ClO 2 Au(ClO 4 ) 4 . Synthesis and Molecular and Crystal Structure Analysis

✍ Scribed by Cunin, Frédérique; Deudon, Catherine; Favier, Frédéric; Mula, Bernard; Pascal, Jean Louis

Book ID
126029458
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
15 KB
Volume
41
Category
Article
ISSN
0020-1669

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Perchlorato Complexes of Rare-Earth Elem
Perchlorato Complexes of Rare-Earth Elements: Syntheses and Crystal Structures of Lu(ClO4)3 · 3 H2O, Er(ClO4)3 · H2O, and Sc(OH)(ClO4)2 · H2O
✍ Mathias S. Wickleder 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 German ⚖ 181 KB 👁 2 views

Single crystals of Lu(ClO 4 ) 3 ´3 H 2 O were obtained by slow dehydration of Lu(ClO 4 ) 3 ´6 H 2 O at 140 °C under flowing argon. The compound crystallizes in the triclinic crystal system (P1, Z = 2, a = 750.3(1), b = 838.4(1), c = 1054.6(2) pm, a = 79.77(2)°, b = 79.18(2), c = 63.83(2), R all = 0.