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FICA, a new chiral derivatizing agent for determining the absolute configuration of secondary alcohols by 19F and 1H NMR spectroscopies

✍ Scribed by Takahashi, Tamiko; Kameda, Hiroaki; Kamei, Tomoyo; Koyanagi, Jyunichi; Pichierri, Fabio; Omata, Kenji; Ishizaki, Miyuki; Nakamura, Hiroshi

Book ID
120969702
Publisher
Elsevier Science
Year
2013
Tongue
English
Weight
928 KB
Volume
24
Category
Article
ISSN
0957-4166

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A new approach for the determination of
A new approach for the determination of the absolute configuration of secondary alcohols by 1H NMR with O-substituted mandelate derivatives
✍ Isabelle Chataigner; Jacques Lebreton; Didier Durand; AndrΓ© Guingant; Jean Villi πŸ“‚ Article πŸ“… 1998 πŸ› Elsevier Science 🌐 French βš– 223 KB

It is shown that the cheap and easily prepared mandelic acid esters (or their OAc analogues) are best suited than the expensive, although usually employed, OMe mandelic acid esters to assess both the enantiomeric excesses and absolute configurations of secondary alcohols.