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Fenton oxidation of hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) and octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)

✍ Scribed by Kyung-Duk Zoh; Michael K. Stenstrom

Book ID
117242453
Publisher
IWA Publishing
Year
2002
Tongue
English
Weight
293 KB
Volume
36
Category
Article
ISSN
0043-1354

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New adducts of octahydro-1,3,5,7-tetrani
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## Abstract A new series of relatively stable adducts of octahydro‐1,3,5,7‐tetranitro‐1,3,5,7‐tetrazocine (HMX) with derivatives of pyridine‐N‐oxide were prepared. In addition, relative stable new adducts of HMX were prepared with 5‐membered, 6‐membered, and condensed‐ring heterocyclic compounds. M

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## Abstract Various methods of preparation of the different polymorphs of HMX have been evaluated. Infrared and Raman spectra have been used to differentiate the polymorphs and understand their conformational behaviour. Possible conformation of the γ form has been suggested.

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H NMR spectra of the energetic materials a -h e x ~y d r o -1 , 3 , 5 -~~o -s -~~e (RDX) and the a-, 8-, yand S-polymorphs of octahydro-1,3,5,7-te~tro-l,3,5,7-tetrazocine (HMX) have been obtained in the solid phase. Primary and secondary dipole-dipole interactions can be observed, which allows calcu