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Fe(CO)5-initiated reaction of CCl4with 1,1-dichloro-5-cyano-1-pentene and 1,1,5-trichloro-1-pentene

✍ Scribed by N. V. Kruglova; V. I. Dostovalova; R. Kh. Freidlina


Book ID
112449024
Publisher
Springer
Year
1980
Tongue
English
Weight
436 KB
Volume
29
Category
Article
ISSN
1573-9171

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Synthesis of 1-pentene-4-14C and 1-pente
✍ P. Ph. H. L. Otto; B. van Zanten πŸ“‚ Article πŸ“… 2010 πŸ› Elsevier Science 🌐 English βš– 222 KB

## Abstract 1‐Pentene‐4‐^14^C and 1‐pentene‐5‐^14^C were obtained in one single step from iodoethane‐1‐^14^C and iodoethane‐2‐^14^C, respectively, by reaction with allylmagnesium chloride in tetrahydrofurfuroxytetrahydropyran (TFTP) as solvent. The synthesis was carried out on a twenty mmoles scale