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Fast atom bombardment mass spectrometry of the large oligopeptides melittin, glucagon and the B chain of bovine insulin

✍ Scribed by Michael Barber; Robert S. Bordoli; R. Donald Sedgwick; Andrew N. Tyler; George V. Garner; Derek B. Gordon; Lee W. Tetler; Robert C. Hider

Book ID
101755709
Publisher
John Wiley and Sons
Year
1982
Tongue
English
Weight
283 KB
Volume
9
Category
Article
ISSN
1076-5174

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New methodology for identifying and locating crosslinkages in peptides is described. Pepsin is used to cleave insulin and B-chain dimers of insulin into fragments under conditions which retain the original peptide crosslinkages. After partial separation by HPLC, the peptides are analyzed by fast ato