Fast acquisition of extensive X-ray diffraction patterns of a gas–liquid interface in grazing-incidence geometry
✍ Scribed by Konovalov, Oleg V.; Vorobiev, Alexei A.
- Book ID
- 119982270
- Publisher
- International Union of Crystallography
- Year
- 2012
- Tongue
- English
- Weight
- 808 KB
- Volume
- 46
- Category
- Article
- ISSN
- 0021-8898
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📜 SIMILAR VOLUMES
## Abstract A grazing‐incidence X‐ray‐diffraction (GIXD) study of the self‐assembly, on water, of nonracemic __γ__‐stearyl glutamic acid (pure or as a mixture with racemic or (__S__)‐1,2‐dipalmitoyl‐glycero‐3‐phosphoethanolamine (DPPE)) demonstrated a phase separation of the __α__‐amino acid amphip
## COMMUNICATIONS be performed under argon. After drying the combined organic layers over sodium sulfate and removing the solvent, the crude product was obtained, which was purified by flash chromatography on silica gel (50 g), Subsequent recrystallization provided compounds 4 in analytically pure