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Structure Determination in the Twilight Region Between Monolayers and 3-D Crystals; a Grazing Incidence X-Ray Diffraction Study of Nanocrystalline Aggregates of α,ω-Docosanediol at the Air–Water Interface

✍ Scribed by Jaroslaw Majewski; Ron Edgar; Dr. Ronit Popovitz-Biro; Dr. Kristian Kjaer; Dr. Wim G. Bouwman; Prof. Jens Als-Nielsen; Prof. Meir Lahav; Professor Leslie Leiserowitz

Publisher: John Wiley and Sons
Year: 1995
Tongue: English
Weight: 528 KB
Volume: 34
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.199506491

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✦ Synopsis

COMMUNICATIONS

be performed under argon. After drying the combined organic layers over sodium sulfate and removing the solvent, the crude product was obtained, which was purified by flash chromatography on silica gel (50 g), Subsequent recrystallization provided compounds 4 in analytically pure form.

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✍ Isabelle Weissbuch; Irina Rubinstein; Markus J. Weygand; Kristian Kjaer; Leslie 📂 Article 📅 2003 🏛 John Wiley and Sons 🌐 German ⚖ 259 KB

## Abstract A grazing‐incidence X‐ray‐diffraction (GIXD) study of the self‐assembly, on water, of nonracemic __γ__‐stearyl glutamic acid (pure or as a mixture with racemic or (__S__)‐1,2‐dipalmitoyl‐glycero‐3‐phosphoethanolamine (DPPE)) demonstrated a phase separation of the __α__‐amino acid amphip