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Facile Synthetic Methods for the Diversification of Catena-Polyphosphorus Cations

✍ Scribed by Neil Burford; C. Adam Dyker; Andreas Decken

Book ID
101534838
Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
133 KB
Volume
117
Category
Article
ISSN
0044-8249

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Facile Synthetic Methods for the Diversi
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✍ Neil Burford; C. Adam Dyker; Andreas Decken πŸ“‚ Article πŸ“… 2005 πŸ› John Wiley and Sons 🌐 English βš– 133 KB

The propensity for phosphorus to form catenated compounds is evidenced by the extensive arrays of structurally characterized polyphosphines [1, 2] and homopolyatomic anions reported. [3] In contrast, comprehensively characterized polyphosphorus cations are limited to phosphinophosphonium 1, [4][5][6

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A new, convenient and efficient synthetic method for the construction of 1,3-oxathiolan-2-ylidenes via sodium borohydride reduction of the addition product of dithiocarbamic acid esters with a-bromoketones under basic conditions is reported. This method is general and applicable to a range of system

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