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Facile synthesis of isocampholenic acids by the rearrangement of camphor derivatives

โœ Scribed by Biggs, Robyn Aryn; Ogilvie, William W.

Book ID
118228878
Publisher
Elsevier Science
Year
2013
Tongue
French
Weight
245 KB
Volume
69
Category
Article
ISSN
0040-4020

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A facile synthesis of primary amines fro
A facile synthesis of primary amines from carboxylic acids by the curtius rearrangement
โœ Todd L. Capson; C.Dale Poulter ๐Ÿ“‚ Article ๐Ÿ“… 1984 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 197 KB

Ab4tic.Z . 2-Trimethylsilylethanol was used to trap isocyanates produced by the Curtius rearrangement of acyl azides and the resulting trimethylsilylethyl carbamates were readily cleaved with tetra-n-butylammonium fluoride to liberate the primary amines.