Evaluation of gas chromatograph packings for the separation of butyric acid from serum-catalyzed hydrolysis of ethyl butyrate
โ Scribed by Premysl Mares; Oyin Somobin; Jiri Coupek
- Publisher
- Elsevier Science
- Year
- 1978
- Tongue
- English
- Weight
- 247 KB
- Volume
- 90
- Category
- Article
- ISSN
- 0003-2697
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โฆ Synopsis
BIOCHEMISTRY 90. 824-828 (1978) ' Abbreviations used: gc, gas chromatograph: fid. flame ionization detector; and HETP. height equivalent to theoretical plate.
๐ SIMILAR VOLUMES
The chromatographic problems associated with strong adsorption of halocarbons onto a Chromosorb 107 packed column were eliminated by using multidimensional gas chromotography. The adsorption required rapid temperature programming to elute the halocarbons in a reasonable time, in turn producing peaks
Butyrate and longer-chain fatty acids are quantitatively extracted from an incubation medium and separated from ["Clacetate with a recovery of 93.6 f 2.3 and 96.7 \* 2.4% for butyrate and palmitate, respectively. Butyrate and longer-chain fatty acids are methylated and prepared for radio gas chromat