✦ LIBER ✦

Quantitative extraction and separation from [1-14C]acetate and preparation for radio gas chromatography of microgram amounts of a 14C-labeled mixture of butyrate and longer-chain-length fatty acids

✍ Scribed by J. Knudsen; J.Krogh Hansen; I. Grunnet

Publisher: Elsevier Science
Year: 1981
Tongue: English
Weight: 331 KB
Volume: 112
Category: Article
ISSN: 0003-2697
DOI: 10.1016/0003-2697(81)90279-7

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✦ Synopsis

Butyrate and longer-chain fatty acids are quantitatively extracted from an incubation medium and separated from ["Clacetate with a recovery of 93.6 f 2.3 and 96.7 * 2.4% for butyrate and palmitate, respectively. Butyrate and longer-chain fatty acids are methylated and prepared for radio gas chromatography with a recovery of butyrate and palmitate from the incubation medium of 90.7 f 1.8% and 93.5 k 2.3%, respectively.