All interatomic distances in the title compound, C~13~H~15~N~3~O~2~S, are normal. The 1,2,4-triazole ring is planar and is inclined at 46.50 (6)° to the phenyl ring. The ethoxycarbonylmethyl group is also close to being planar and is inclined at 87.54 (9)° to the 1,2,4-triazole ring. The crystal was
Ethyl 2-(4-phenyl-1H-1,2,3-triazol-1-yl)acetate
✍ Scribed by Zhang, Xiao-Ru ;Xu, Min-Hua ;Li, Xue-Mei ;Zhang, Shu-Sheng
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 100 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.
In the molecule of the title compound, C 21 H 18 N 4 O 2 S, all of the rings are individually planar. In the crystal structure, the molecules are linked by intermolecular N-HÁ Á ÁO hydrogen bonds, forming an infinite chain.
In the crystal structure of the title compound, C 15 H 14 N 4 , all three aromatic rings, viz. 1,2,4-triazole, pyridine and benzene. The crystal structure shows that all three rings are not coplanar.
The title compound, C 28 H 24 N 6 O 4 , crystallizes with one halfmolecule in the asymmetric unit, the other half being generated by a center of inversion. In the crystal structure, molecules are linked into ribbons along the a axis by weak C-HÁ Á ÁN hydrogen bonds.