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Ethyl 2-{2-[(1-methyl-2-phenyl-1H-indol-3-yl)diazen­yl]thia­zol-4-yl}­acetate

✍ Scribed by Seferoğlu, Zeynel ;Hökelek, Tuncer ;Şahin, Ertan ;Saylam, Aytül ;Ertan, Nermin


Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
116 KB
Volume
62
Category
Article
ISSN
1600-5368

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In the molecule of the title compound, C 21 H 18 N 4 O 2 S, all of the rings are individually planar. In the crystal structure, the molecules are linked by intermolecular N-HÁ Á ÁO hydrogen bonds, forming an infinite chain.

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In the title molecule, C 22 H 18 N 4 O, all of the rings and the indole system are individually planar. In the crystal structure, molecules are linked by intermolecular N-HÁ Á ÁO hydrogen bonds, forming infinite chains running along the [001] direction.

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In the molecular structure of the title compound, C~8~H~7~N~5~O~3~S, the thiazole ring is oriented with respect to the barbituric acid ring at a dihedral angle of 5.14 (9)°. In the crystal structure, intermolecular N—H...N and N—H...O hydrogen bonds link the molecules, forming a layer parallel to th

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.116 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.