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ESR and ESE study of conformational transitions of the cyclic radical (CH2)4>ĊCO2−in the solid phase

✍ Scribed by S. A. Dzyuba; O. A. Shushakov; Yu. D. Tsvetkov

Publisher
SP MAIK Nauka/Interperiodica
Year
1984
Tongue
English
Weight
518 KB
Volume
24
Category
Article
ISSN
0022-4766

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✍ Herbert Rubin; Hanns Fischer 📂 Article 📅 1996 🏛 John Wiley and Sons 🌐 German ⚖ 686 KB

All arrangements and procedures for steady-state and time-resolved ESR were as described in [4]. The radicals Me,C and Me3C02CCH, were generated by photolysis of the corresponding disubstituted ketones. These undergo type-I cleavage from a short-lived triplet state followed by a fast decarbonylation