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Enzymatic synthesis of 3-deoxy-D-manno-2-octulosonic acid and analogues: a new approach by a non metabolic pathway

✍ Scribed by Christine Guérard; Colette Demuynck; Jean Bolte

Publisher
Elsevier Science
Year
1999
Tongue
French
Weight
165 KB
Volume
40
Category
Article
ISSN
0040-4039

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Synthesis of methyl pyranosides and furanosides of 3-deoxy-d-manno-oct-2-ulosonic acid (KDO) by acid-catalysed solvolysis of the acetylated derivatives
✍ Paul A. McNicholas; Michael Batley; John W. Redmond 📂 Article 📅 1986 🏛 Elsevier Science 🌐 English ⚖ 838 KB

Treatment of methyl 2,4,5,7,8-penta-O-acetyl-3-deoxy-cr-D-manno-oct-2ulopyranosonic acid, or its methyl ester, with refluxing methanolic O.lM hydrogen chloride for 16 h gave 95% of methyl (methyl 3-deoxy-a-D-manno-act-2-ulopyranosid)onate. Acetylation of the methyl ester of 3-deoxy-D-manno-act-2ulo