## Abstract Guanylurea nitrate (GUN) and guanylurea perchlorate (GUP) were prepared from cyanoguanidine (CG) and concentrated nitric or perchloric acid, respectively. Both compounds were fully characterized by analytical and spectroscopic methods. Crystals of GUP were grown from water, and its crys
Energetic Nitrate, Perchlorate, Azide and Azolate Salts of Hexamethylenetetramine
✍ Scribed by Hong Xue; Haixiang Gao; Brendan Twamley; Jean’ne M. Shreeve
- Publisher
- John Wiley and Sons
- Year
- 2006
- Tongue
- English
- Weight
- 142 KB
- Volume
- 2006
- Category
- Article
- ISSN
- 1434-1948
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Urotropinium nitrate, N-methylurotropinium azide, dinitramide and azotetrazolate salts have been prepared and fully characterized by analytical and spectoscopic ( 1 H, 13 C, 14 N NMR, IR, Raman) methods. The structures of all four compounds have been determined using X-ray diffraction techniques and
For both structures all hydrogens were located in difference Fourier syntheses. The structures were refined by least-squares methods (OWLS ' ' 1 ; scale factor, isotropic extinction parameter, position parameters, anisotropic thermal parameters for non-Hatoms, isotropic thermal parameters for H) to