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Enantiospecific Synthesis of the Phospholipase A2 Inhibitor (-)-Cinatrin B.

โœ Scribed by Anthony N. Cuzzupe; Romina Di Florio; Mark A. Rizzacasa


Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
33
Category
Article
ISSN
0931-7597

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Synthesis of a tritium labelled phosphol
โœ A. S. Culf; H. Morimoto; P. G. Williams; W. J. S. Lockley; W. U. Primrose; J. R. ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 490 KB ๐Ÿ‘ 2 views

A tritium labelled phospholipase A2 (PLA2) amide analogue inhibitor was prepared by the reduction of an alkene precursor. Diimide, heterogeneous and homogeneous metal catalyzed reduction methods were assessed for their suitability for the preparation of a tritiated ligand for 3H NMR spectroscopic st