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Enantiomerically Pure Palladacycles Derived from β-Ketosulfoxides

✍ Scribed by Prof. José L. García-Ruano; Ana M. González; Dr. Isabel López-Solera; Prof. José R. Masaguer; Prof. Carmen Navarro-Ranninger; Dr. Paul R. Raithby; Dr. Jesús H. Rodríguez

Publisher
John Wiley and Sons
Year
1995
Tongue
English
Weight
392 KB
Volume
34
Category
Article
ISSN
0044-8249

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We have reported' the transformation of 2,3-unsaturated glycosides 1 into the respective 2,3-dideoxyhex-2-enono-1 ,Slactones 2 by oxidation with 30% hydrogen peroxide in the presence of molybdenum trioxide as catalyst, followed by dehydration of the resulting hydroperoxide 3. Other syntheses of 2 ha