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Enantiomeric separation of 2-aryloxyalkyl- and 2-arylalkyl-2-aryloxyacetic acids on a Penicillin G Acylase-based chiral stationary phase: Influence of the chemical structure on retention and enantioselectivity

✍ Scribed by Caterina Temporini; Enrica Calleri; Giuseppe Fracchiolla; Giuseppe Carbonara; Fulvio Loiodice; Antonio Lavecchia; Paolo Tortorella; Gloria Brusotti; Gabriella Massolini

Book ID: 118477615
Publisher: Elsevier Science
Year: 2007
Tongue: English
Weight: 980 KB
Volume: 45
Category: Article
ISSN: 0731-7085
DOI: 10.1016/j.jpba.2007.06.005

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## Abstract A series of structurally related 2‐aryloxy‐2‐arylacetic acids (**1–3, 5–16**) together with a thioisostere derivative (**4**) have been synthesized and characterized by GC‐MS and ^1^H NMR. The designed compounds were analyzed on a Penicillin G Acylase chiral stationary phase (PGA‐CSP) a