Empirical determination of the absolute configuration of small chiral molecules using natural abundance 2H NMR in chiral liquid crystals
β Scribed by Ziani, Latifa; Lesot, Philippe; Meddour, Abdelkhrim; Courtieu, Jacques
- Book ID
- 121009847
- Publisher
- Royal Society of Chemistry
- Year
- 2007
- Tongue
- English
- Weight
- 341 KB
- Volume
- 45
- Category
- Article
- ISSN
- 1359-7345
- DOI
- 10.1039/B711493A
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## Abstract A highβresolution, phaseβsensitive, natural abundance __F__~2~βcoupled ^1^Hβ^13^C HSQC (F2HSQC) NMR experiment was developed to measure simultaneously both ^__n__^__D__~HH~ and ^1^__D__~CH~ residual dipolar couplings (RDCs) of small molecules present in a chiral polypeptide liquid cryst