Elimination of resonance offset effects in rotational-echo, double-resonance NMR
β Scribed by Terry Gullion; Jacob Schaefer
- Publisher
- Elsevier Science
- Year
- 1991
- Weight
- 306 KB
- Volume
- 92
- Category
- Article
- ISSN
- 0022-2364
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π SIMILAR VOLUMES
## REDOR is a magic-angle spinning experiment for measuring internuclear distances between heteronuclear spin pairs. The basic principles of the REDOR technique are presented. The experimental requirements necessary for quantitative REDOR measurements are also provided.
The spin density matrix formalism has been applied to rotational-echo double-resonance (REDOR), transferred-echo double-resonance (TEDOR) and two-dimensional (2D) TEDOR experiments in order to obtain an expression for the signal intensities. TEDOR spectra of lSN-labeled glycine were measured with di