✦ LIBER ✦

Electroreduction of triphenylphosphine dichloride and the efficient one-pot reductive conversion of phosphine oxide to triphenylphosphine

✍ Scribed by Tomotake Yano; Manabu Kuroboshi; Hideo Tanaka

Book ID: 104097200
Publisher: Elsevier Science
Year: 2010
Tongue: French
Weight: 546 KB
Volume: 51
Category: Article
ISSN: 0040-4039
DOI: 10.1016/j.tetlet.2009.11.115

No coin nor oath required. For personal study only.

✦ Synopsis

Electroreduction of triphenylphosphine dichloride in acetonitrile was performed successfully in an undivided cell fitted with an aluminium sacrificial anode and a platinum cathode. Further, the one-pot transformation of triphenylphosphine oxide to triphenylphosphine was achieved successfully by the treatment of triphenylphosphine oxide in acetonitrile with oxalyl chloride and subsequent electrochemical reduction.

📜 SIMILAR VOLUMES

Three-Component Reaction of Triphenylpho

Three-Component Reaction of Triphenylphosphine, Dialkyl Acetylenedicarboxylate, and 2-Aminothiazole or 2-Aminobenzothiazole in the Presence of Arylglyoxals: An Efficient One-Pot Synthesis of Highly Functionalized Pyrroles

✍ Anary-Abbasinejad, Mohammad; Farashah, Hamidreza Dehghanpour; Hassanabadi, Alire 📂 Article 📅 2012 🏛 Taylor and Francis Group 🌐 English ⚖ 274 KB

ChemInform Abstract: Three-Component Rea

ChemInform Abstract: Three-Component Reaction of Triphenylphosphine, Dialkyl Acetylenedicarboxylate, and 2-Aminothiazole or 2-Aminobenzothiazole in the Presence of Arylglyoxals: An Efficient One-Pot Synthesis of Highly Functionalized Pyrroles.

✍ Mohammad Anary-Abbasinejad; Hamidreza Deghanpour Farashah; Alireza Hassanabadi; 📂 Article 📅 2012 🏛 John Wiley and Sons ⚖ 29 KB

CuSO4 as a Mild, Green, and Efficient Ca

CuSO4 as a Mild, Green, and Efficient Catalyzed for the One-Pot Conversion of THP Ethers to Acetates.

✍ Karim Asadolah; Majid M. Heravi 📂 Article 📅 2007 🏛 John Wiley and Sons ⚖ 17 KB 👁 2 views

One-pot conversion of CO2 and glycerol t

One-pot conversion of CO2 and glycerol to value-added products using propylene oxide as the coupling agent

✍ Ma, Jun; Song, Jinliang; Liu, Huizhen; Liu, Jinli; Zhang, Zhaofu; Jiang, Tao; Fa 📂 Article 📅 2012 🏛 Royal Society of Chemistry 🌐 English ⚖ 167 KB

ZrCl4 as a mild and efficient catalyst f

ZrCl4 as a mild and efficient catalyst for the one-pot conversion of TBS and THP ethers to acetates

✍ Ch.Sanjeeva Reddy; G Smitha; S Chandrasekhar 📂 Article 📅 2003 🏛 Elsevier Science 🌐 French ⚖ 184 KB

A mild, efficient and chemoselective method has been developed for the direct transformation of tert-butyldimethylsilyl and tetrahydropyranyl protected alcohols into the corresponding acetates with acetic anhydride and zirconium(IV) chloride as the catalyst in acetonitrile, in a one-pot reaction wit

ZrCl4 as a Mild and Efficient Catalyst f

ZrCl4 as a Mild and Efficient Catalyst for the One-Pot Conversion of TBS and THP Ethers to Acetates.

✍ Ch. Sanjeeva Reddy; G. Smitha; S. Chandrasekhar 📂 Article 📅 2003 🏛 John Wiley and Sons ⚖ 137 KB 👁 2 views