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Electrolytic preconcentration in instrumental analysis

✍ Scribed by Roman E. Sioda; Graeme E. Batley; Walter Lund; Joseph Wang; Steven C. Leach

Book ID
118994673
Publisher
Elsevier Science
Year
1986
Tongue
English
Weight
1016 KB
Volume
33
Category
Article
ISSN
0039-9140

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Anodic dissolution of milligram amounts of the sample and removal of most of the dissolved silver are done simultaneously by electrolysis using the sample as anode, a platinum cathode controlled at -0.25 V vs. SCE and 1 ml of 0.08 M nitric acid-O.001 M sutphuric acid as electrolyte. Silver remaining