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Electrochemical reduction of vicinal dinitro compounds

✍ Scribed by Bowyer, Walter J.; Evans, Dennis H.

Book ID: 120224724
Publisher: American Chemical Society
Year: 1988
Tongue: English
Weight: 817 KB
Volume: 53
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00257a008

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Part 4. Synthesis of Compounds Containing Vicinal gem-Dinitro Groups. -Nitration of β-methyl-γ,γ-dinitroketones (III) and (V) proceeds by C-C bond cleavage to afford compounds (IV) and (VI), resp., containing two vicinal gem-dinitro groups. The tetranitrohexanoic acid (VI) is used for the synthesis