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Electrochemical Parametrization in Sandwich Complexes of the First Row Transition Metals

✍ Scribed by Lu, Shuangxing; Strelets, Vladimir V.; Ryan, Matthew F.; Pietro, William J.; Lever, A. B. P.

Book ID
125808992
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
474 KB
Volume
35
Category
Article
ISSN
0020-1669

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## Abstract Lithiated 4‐methyl‐2‐[(trimethylsilyl)amino]pyridine (Ap^TMS^H) undergoes a salt metathesis reaction with [ScCl~3~(thf)~3~] and FeCl~3~, at low temperature in thf, to yield the homoleptic complexes [Sc(Ap^TMS^)~3~] (1) and [Fe(Ap^TMS^)~3~] (2). An analogous reaction with MnCl~2~, CoCl~2