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Late First-Row Transition-Metal Complexes of Texaphyrin

✍ Scribed by Hannah, Sharon; Lynch, Vincent; Guldi, Dirk M.; Gerasimchuk, Nikolay; MacDonald, Charles L. B.; Magda, Darren; Sessler, Jonathan L.

Book ID
126162317
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
184 KB
Volume
124
Category
Article
ISSN
0002-7863

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## Abstract Lithiated 4‐methyl‐2‐[(trimethylsilyl)amino]pyridine (Ap^TMS^H) undergoes a salt metathesis reaction with [ScCl~3~(thf)~3~] and FeCl~3~, at low temperature in thf, to yield the homoleptic complexes [Sc(Ap^TMS^)~3~] (1) and [Fe(Ap^TMS^)~3~] (2). An analogous reaction with MnCl~2~, CoCl~2