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Electrochemical oxidation of phenyldisulfide in acetonitrile medium

โœ Scribed by Gino Bontempelli; Franco Magno; Gian-Antonio Mazzocchin

Publisher
Elsevier Science
Year
1973
Weight
584 KB
Volume
42
Category
Article
ISSN
0022-0728

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Several methods have been suggested for preparing pure, anhydrous acetonitrile for electrochemical purposes 1. All are satisfactory, but there can be a great difference between a freshly distilled solvent and the solution containing the supporting electrolyte. The transfer of the solvent into the ce

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Electrochemical oxidation of a biphenyl mercaptal in acetonitrile
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This note reports on the electrochemical oxidation in acetonitrile of bis-(phenylthio)-methane, a biphenyl mercaptal. In the presence of either sodium or tetraethylammonium perchlorate this compound is cleanly oxidized to diphenyldisulfide and formaldehyde at a platinum electrode. This result is uni