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Electrochemical and spectroscopic study of the addition of several nucleophiles to 1,2,5-thiadiazole 1,1-dioxide derivatives

✍ Scribed by Silvia Lucía Aimone; José Alberto Caram; María Virginia Mirífico; Enrique Julio Vasini


Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
122 KB
Volume
13
Category
Article
ISSN
0894-3230

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Selected 1,4-and 1,5-benzoheterazepinones, prepared by the Schmidt rearrangement of flavanone analogues, were converted to the corresponding thiolactam derivatives using phosphorus pentasulfide. The proton and carbon chemical shifts of the thiolactam derivatives are compared with those of their lact