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EFFICIENT SYNTHESIS OF NEW NITROGEN DONOR CONTAINING TRIPODS UNDER MICROWAVE IRRADIATION AND WITHOUT SOLVENT

โœ Scribed by Touzani, Rachid; Ramdani, Abdelkrim; Ben-Hadda, Taibi; El Kadiri, Sghir; Maury, Olivier; Bozec, Hubert Le; Dixneuf, Pierre H.


Book ID
121512274
Publisher
Taylor and Francis Group
Year
2001
Tongue
English
Weight
116 KB
Volume
31
Category
Article
ISSN
0039-7911

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2,3-Dihydro-1H-1,5-benzodiazepines have been synthesized in solvent-free conditions from o-phenylenediamines and ketones in the presence of a catalytic amount of acetic acid, under microwave irradiation. This method is a very easy, rapid and high yielding reaction for the synthesis of 1,5-benzodiaze