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Efficient Solvent-Free Syntheses of [2]- and [4]Rotaxanes

✍ Scribed by Sheng-Yao Hsueh; Kuang-Wei Cheng; Chien-Chen Lai; Sheng-Hsien Chiu

Book ID: 102728137
Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 512 KB
Volume: 47
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.200800530

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Three dumbbell-shaped compounds incorporating terminal chains of the templates influences the efficiencies of the template-directed syntheses. Rotaxane formation occurs only triisopropylsilyl stoppers, connected to a central 1,5dioxynaphthalene recognition site by [-CH 2 CH 2 O-] n spacers if n Ͼ 1