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Efficient Intermolecular [2 + 2 + 2] Alkyne Cyclotrimerization in Aqueous Medium Using a Ruthenium(IV) Precatalyst.

✍ Scribed by Victorio Cadierno; Sergio E. Garcia-Garrido; Jose Gimeno

Publisher: John Wiley and Sons
Year: 2007
Weight: 29 KB
Volume: 38
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200715091

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✦ Synopsis

Abstract

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Efficient Tandem Process for the Catalyt

Efficient Tandem Process for the Catalytic Deprotection of N-Allyl Amides and Lactams in Aqueous Media: A Novel Application of the Bis(allyl)-Ruthenium(IV) Catalysts [Ru(η3:η2:η3-C12 H18)Cl2] and [{Ru(η3:η3-C10H16) (μ-Cl)Cl}2].

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Efficient Tandem Process for the Catalyt

Efficient Tandem Process for the Catalytic Deprotection of N-Allyl Amides and Lactams in Aqueous Media: A Novel Application of the Bis(allyl)–Ruthenium(IV) Catalysts [Ru(η3:η2:η3-C12H18)Cl2] and [{Ru(η3:η3-C10H16)(μ-Cl)Cl}2]

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## Abstract An operationally simple and highly efficient methodology for the removal of the allyl protecting group in amides and lactams has been developed by using the commercially available bis(allyl)–ruthenium(IV) catalysts [Ru(η^3^:η^2^:η^3^‐C~12~H~18~)Cl~2~] (C~12~H~18~=dodeca‐2,6,10‐triene‐1,