Efficient heteronuclear dipolar decoupling in solid-state NMR using frequency-swept SPINAL sequences
✍ Scribed by C. Vinod Chandran; Thomas Bräuniger
- Book ID
- 108184960
- Publisher
- Elsevier Science
- Year
- 2009
- Tongue
- English
- Weight
- 568 KB
- Volume
- 200
- Category
- Article
- ISSN
- 1090-7807
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## Abstract Recently, a pulse scheme for heteronuclear spin decoupling in solid‐state NMR, called swept‐frequency two‐pulse phase modulation (SW~f~‐TPPM), was introduced which outperforms the standard TPPM and small phase incremental alteration (SPINAL) schemes. It has also been shown that the freq
## Abstract Heteronuclear dipolar decoupling is an essential requirement for extracting structural information from the ^13^C NMR spectra of liquid crystals. Efficient schemes for heteronuclear dipolar decoupling in such systems are formulated here by supercycling SW~f~‐TPPM, a sequence introduced