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Supercycled SWf-TPPM sequence for heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance

✍ Scribed by Cyril Augustine; Narayanan D. Kurur


Book ID
108185037
Publisher
Elsevier Science
Year
2011
Tongue
English
Weight
579 KB
Volume
209
Category
Article
ISSN
1090-7807

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Heteronuclear dipolar decoupling in liqu
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## Abstract Heteronuclear dipolar decoupling is an essential requirement for extracting structural information from the ^13^C NMR spectra of liquid crystals. Efficient schemes for heteronuclear dipolar decoupling in such systems are formulated here by supercycling SW~f~‐TPPM, a sequence introduced

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## Abstract Recently, a pulse scheme for heteronuclear spin decoupling in solid‐state NMR, called swept‐frequency two‐pulse phase modulation (SW~f~‐TPPM), was introduced which outperforms the standard TPPM and small phase incremental alteration (SPINAL) schemes. It has also been shown that the freq