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Efficient and Scalable Method for the Selective Alkylation and Acylation of Secondary Amines in the Presence of Primary Amines

✍ Scribed by Laduron, Frédéric; Tamborowski, Vanessa; Moens, Luc; Horváth, András; De Smaele, Dirk; Leurs, Stef

Book ID
118118272
Publisher
American Chemical Society
Year
2005
Tongue
English
Weight
51 KB
Volume
9
Category
Article
ISSN
1083-6160

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Selective benzoylation of primary amines
Selective benzoylation of primary amines in the presence of secondary amines
✍ Tao Wang; Zhongxing Zhang; Nicholas A. Meanwell 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 120 KB

Compounds containing both primary and secondary amine moieties in the same molecule were treated sequentially with two equivalents of n-butyllithium at room temperature, two equivalents of TMSCI, one equivalent of nbutyllithium and one equivalent of benzoyl chloride, to afford mono-benzoylated diami