The polymorphic phase transitions of Bi 2 Te 4 O 11 have been investigated using X-ray powder diffraction (XPD), selected area electron diffraction (SAED), and differential scanning calorimetry (DSC) in the 25-730Β°C range. The metastable cubic modification, which forms under fast crystalization of t
Effect of Polymer Matrix on the Phase Transitions of CuFe2O4
β Scribed by S. Roy; J. Ghose
- Publisher
- Elsevier Science
- Year
- 1999
- Tongue
- English
- Weight
- 118 KB
- Volume
- 144
- Category
- Article
- ISSN
- 0022-4596
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β¦ Synopsis
The effect of a polymer matrix on phase transitions in CuFe 2 O 4 spinel oxide has been studied. XRD results show that cubic CuFe 2 O 4 is obtained by quenching from 1173 K, while with CuFe 2 O 4 -PEEK composite samples, the cubic form is obtained by quenching from considerably lower temperatures (:733 K). The change in resistivity with temperature of the quenched composite samples shows that the cubic samples quenched from < 1173 K undergo several phase changes during heating. Measurements of thermoelectric power indicate that the composite samples quenched from 41073 K show n-type conduction, and the sample quenched from 1173 K shows p-type conduction.
π SIMILAR VOLUMES
Raman and IR studies of a single orthorhombic crystal and of polycrystalline trigonal RbIn(MoO 4 ) 2 were performed at ambient temperature. The observed vibrational modes were assigned to the respective motions of atoms in the unit cells. It was shown that the first-order D 3d 3 β D 2h 16 phase tran