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Effect of Cobalt-59 Self-Decoupling on the Solid-State 31 P CP/MAS NMR Spectra of Cobaloximes

✍ Scribed by Schurko, Robert W.; Wasylishen, Roderick E.; Nelson, John H.

Book ID: 121371414
Publisher: American Chemical Society
Year: 1996
Tongue: English
Weight: 290 KB
Volume: 100
Category: Article
ISSN: 0022-3654
DOI: 10.1021/jp960563q

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## Abstract An investigation of bis(diphenylphosphino)methane dioxide (dppm dioxide), __cis__‐[PtCl~2~(PPh~3~)~2~] __cis__‐[PtCl~2~{P(__p__‐C~6~H~4~Cl)~3~}~2~] and __cis__‐[PtBr~2~(PPh~3~)~2~] by solid‐state CP/MAS ^31^P NMR spectroscopy, x‐ray powder diffraction and ^1^H, ^13^C{^1^H} and ^31^P{^1^