Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A R factor = 0.049 wR factor = 0.131 Data-to-parameter ratio = 12.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
(E)-1-[3-Ethoxy-4-(4-methylbenzenesulfonyloxy)benzylidene]-2-(4-nitrophenyl)hydrazine acetonitrile solvate
✍ Scribed by Chen, Xin ;Yu, Ming
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 150 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 21 H 19 N 3 O 6 S, crystallizes with two molecules in the asymmetric unit. The conformations of these non-planar molecules are similar. Intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds help to consolidate the crystal structure.
The structure of (I), with displacement ellipsoids for non-H atoms drawn at the 30% probability level.
In the title compound, C 21 H 19 N 3 O 6 S, the vanillin group makes dihedral angles of 56.00 (7) and 7.22 (8) with the 4-methylbenzene ring and the nitrophenylhydrazine ring, respectively. The crystal packing is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonds and weak, non-classical intermole
The molecule of the title compound, C 20 H 18 N 4 O 6 ÁC 3 H 3 N, is non-planar. The central benzene ring makes dihedral angles of 85.73 (10) and 2.70 (12) with the terminal phenyl ring and the nitrophenylhydrazine mean plane, respectively. An intramolecular N-HÁ Á ÁO hydrogen bond helps to establis