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Dynamic Synthesis of a Macrocycle Containing a Porphyrin and an Electron Donor.

✍ Scribed by Amy L. Kieran; Sofia I. Pascu; Thibaut Jarrosson; Maxwell J. Gunter; Jeremy K. M. Sanders

Book ID
101971244
Publisher
John Wiley and Sons
Year
2005
Weight
8 KB
Volume
36
Category
Article
ISSN
0931-7597

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The antiaromatic macrocycle 2 has been prepared by the reaction of the bipyrrole dialdehyde 1 with hydrazine. In the crystal structure of 2β€’DMSO molecule 2 is nearly planar, the mean deviation of the 28 atoms of the core from the best least-squares plane being 0.227 Γ…. AM1 geometric optimization of