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Dynamic behavior and crystal structures of Pd2(.mu.NS,.eta.2-L)2Cl2(PMe3)2 (L = pyrimidine-2-thiolate, 4-methylpyrimidine-2-thiolate, and methylimidazole-2-thiolate): influence of the N-C-S bond angle on the stability of (heterocyclic 2-thiolato)dipalladium complexes

✍ Scribed by Yap, Glenn P. A.; Jensen, Craig M.

Book ID: 127130012
Publisher: American Chemical Society
Year: 1992
Tongue: English
Weight: 646 KB
Volume: 31
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic00049a020

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## Abstract A series of mono‐ and disubstituted diiron complexes [(μ‐pdt)Fe~2~(CO)~5~L] [pdt = 1,3‐propanedithiolato; L = PMe~3~ (2), PMe~2~Ph (3PPh~3~ (4), P(OEt)~3~ (5)] and [(μ‐pdt)Fe~2~(CO)~4~L~2~] [L = PMe~2~Ph (6), PPh~3~ (7), P(OEt)~3~ (8)] were prepared as Fe‐only hydrogenase‐active‐site mo