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Discovery and crystal structure of a novel chlorocarbon host: perchlorofluorene-9-spirocyclohexa-2′,5′-diene

✍ Scribed by James H. Gall; David D. MacNicol; Paul R. Mallinson; Peter A. Welsh

Book ID: 104228862
Publisher: Elsevier Science
Year: 1985
Tongue: French
Weight: 275 KB
Volume: 26
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)98710-0

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✦ Synopsis

Chlorination of triphenylene

(k) employing a mixture of aluminium trichloride and sulphur monochloride in sulphuryl chloride leads to rearrangement with formation of the title chlorocarbon (2_), a new host, as main product. X-ray crystal structure analyses of the unsolvated spirocycle

(2) as well as of its inclusion compounds with guests benzene and (

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