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Synthesis, characterization and crystal structure of a novel tris(2-aminoethyl) amine copper(II) complex with an asymmetric coordinated 4,5-diazafluorene-9-hydrazine

✍ Scribed by Zhong-Lin Lu; Chun Duan; Yu-Peng Tian; Xiao-Zeng You; Hoong-Kum Fun; Boon-Chuan Yip; Eric Hovestreydt

Publisher: Elsevier Science
Year: 1997
Tongue: English
Weight: 550 KB
Volume: 16
Category: Article
ISSN: 0277-5387
DOI: 10.1016/0277-5387(96)00175-1

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Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OH±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Ê , b = 107.105(3)°,