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Direct solid-phase synthesis and fluorescence labeling of large, monodisperse mannosylated dendrons in a peptide synthesizer

✍ Scribed by Kantchev, Eric Assen B.; Chang, Chung-Chieh; Cheng, Shu-Fang; Roche, Annie-Claude; Chang, Ding-Kwo

Book ID: 120328915
Publisher: Royal Society of Chemistry
Year: 2008
Tongue: English
Weight: 430 KB
Volume: 6
Category: Article
ISSN: 1477-0520
DOI: 10.1039/B719737C

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The efficiency of six different mixing methods for solid-phase organic synthesis was evaluated for the reaction between formylpolystyrene resin and dansylhydrazine by means of single bead IR and fluorescence spectroscopy. The 360° rotating and nitrogen bubbling methods gave highest yields with mild