✦ LIBER ✦
A direct comparison of the mixing efficiency in solid-phase organic synthesis by single bead IR and fluorescence spectroscopy
✍ Scribed by Wenbao Li; Bing Yan
- Book ID
- 104257835
- Publisher
- Elsevier Science
- Year
- 1997
- Tongue
- French
- Weight
- 190 KB
- Volume
- 38
- Category
- Article
- ISSN
- 0040-4039
No coin nor oath required. For personal study only.
✦ Synopsis
The efficiency of six different mixing methods for solid-phase organic synthesis was evaluated for the reaction between formylpolystyrene resin and dansylhydrazine by means of single bead IR and fluorescence spectroscopy. The 360° rotating and nitrogen bubbling methods gave highest yields with mild conditions. O 1997 Elsevier Science Ltd.