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Direct, One-pot Sequential Reductive Alkylation of Lactams/Amides with Grignard and Organolithium Reagents through Lactam/Amide Activation

โœ Scribed by Kai-Jiong Xiao; Jie-Min Luo; Ke-Yin Ye; Yu Wang; Pei-Qiang Huang

Publisher
John Wiley and Sons
Year
2010
Tongue
English
Weight
310 KB
Volume
49
Category
Article
ISSN
0044-8249

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Versatile One-Pot Reductive Alkylation o
Versatile One-Pot Reductive Alkylation of Lactams/Amides via Amide Activation: Application to the Concise Syntheses of Bioactive Alkaloids (ยฑ)-Bgugaine, (ยฑ)-Coniine, (+)-Preussin, and (โˆ’)-Cassine
โœ Kai-Jiong Xiao; Yu Wang; Ke-Yin Ye; Prof. Pei-Qiang Huang ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 254 KB ๐Ÿ‘ 1 views

Scheme 4. Retrosynthetic analysis of (+)-preussin ( ) and (ร€)-cassine (5). Scheme 5. Total synthesis of (+)-preussin (4). Scheme 6. Total synthesis of (ร€)-cassine (5).