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Direct identification of pentoses and hexoses by pyrolysis/capillary gas chromatography

โœ Scribed by D.R. Budgell; E.R. Hayes; R.J. Helleur


Publisher
Elsevier Science
Year
1987
Tongue
English
Weight
681 KB
Volume
192
Category
Article
ISSN
0003-2670

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A sensitive method for the identification of polysaccharides in pharmaceuticals is described. Polysaccharides are isolated by gel filtration and subsequently hydrolysed. The monomeric carbohydrates obtained are transformed into oxime-trimethylsilyl derivatives and analysed by capillary gas chromatog