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Direct fluorination of 2,2,4,4-tetramethylpentane. Sterically protected residual protons?

✍ Scribed by Shimp, L. A.; Lagow, R. J.

Book ID: 126023985
Publisher: American Chemical Society
Year: 1977
Tongue: English
Weight: 285 KB
Volume: 42
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00441a025

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## Abstract 3‐Aryl‐1,2,4‐triazin‐5(2__H__)‐ones 1a‐c react with indoles 2a‐c in trifluoroacetic acid/chloroform or in boiling butanol or acetic acid to give 3‐aryl‐6‐(indolyl‐3)‐1,6‐dihydro‐1,2,4‐triazin‐5(2__H__)‐ones 3a‐g. Oxidation of the dihydro‐1,2,4‐triazin‐5(2__H__)‐ones 3a‐e afforded 6‐(ind