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Direct Conversion of Aromatic Nitro Compounds into Isothiocyanates

✍ Scribed by Dr. G. Ottmann; Dr. E. Kober

Publisher
John Wiley and Sons
Year
1969
Tongue
English
Weight
134 KB
Volume
8
Category
Article
ISSN
0044-8249

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πŸ“œ SIMILAR VOLUMES

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The reaction ofprima~ nitro compounds with isocyanides and isocyanates in the pmsen~ Β’f a base leads to a new preparation ff nitriles. The reaction probably proceeds through the in situ formation of a nitrile oxide followed by a fast oxygen transfer with the isocyanide. Combined with the Knovemgel a

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Treatment of primary nitro groups, in CH2Cl2 at 0 "c. with Sn(SPhM. R3P. and DEAD affords quickly and abnost quantitatively the corresponding n&riles. in a combined process of deoxygenation and delrydration. The same restdt can be obtained, although not so rapidly. uing only R3P (2 eqtdv.) ond DEAD

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