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Dipotassium hexakis({2,2′-[ethane-1,2-diylbis(nitrilo­methyl­idyne)]diphenolato}nickel(II)) tetracyano­nickelate(II) methanol hexasolvate dihydrate

✍ Scribed by Skovsgaard, Signe ;Bond, Andrew D. ;McKenzie, Christine J.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
572 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 180 K Mean '(C±C) = 0.010 A Ê R factor = 0.055 wR factor = 0.145 Data-to-parameter ratio = 13.9

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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{2,2′-[Ethane-1,2-diylbis(nitrilo­methyl
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✍ Wang, Jing ;Zhu, Dong-Sheng ;Shao, Kui-Zhan ;Xu, Lin 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 204 KB

The title compound, [Zn(C 20 H 18 N 2 O 6 )]ÁCH 3 OH, has been synthesized through a one-step procedure in a methanol solvent. The Zn atom exhibits a distorted trigonal prismatic geometry consisting of two imine N-atom donors, two O-atom donors of the phenoxy groups and two O-atom donors of the depr